HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octanoyl chloride → 8-Chloro-N-(1-hydroxyoctylidene)dibenzo[b,f][1,4]oxazepine-10(11H)-carbohydrazonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, hydrazide | HCID 13560461 | — |
| Product | 8-Chloro-N-(1-hydroxyoctylidene)dibenzo[b,f][1,4]oxazepine-10(11H)-carbohydrazonic acid | HCID 217606 | — |
Reaction Steps
The reaction of an alkanoyl halide and the hydrazide is illustrated by contacting 8-chloro-10,11-dihydrodibenz-[b,f][1,4]oxazepine-10-carboxylic acid hydrazide with octanoyl chloride in the presence of sodium bicarbonate to give 1-octanoyl-2-(8-chloro-10,11-dihydrodibenz[b,f][1,4]oxazepine-10-carbonyl)hydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989719 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-0509d29042f6470586f72ebbf940ed2b |
| Source note | uspto-grants-1976_11 |