HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → HCID 22794219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 22794219 | HCID 22794219 | — |
Reaction Steps
A solution of 5.22 grams of the diol in 1,2-dichloroethane was stirred with 63 grams of manganese dioxide in the presence of 50 milligrams of hydroquinone for one hour. After filtration to remove the manganese dioxide, washing with additional dichloroethane and ether, and evaporation of the filtrate at 30°C., there was obtained 3.98 grams of optically active 7(S)-hydroxy-1-dodecen-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989724 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-93894eb8cc914087abd9bd6fe726e45a |
| Source note | uspto-grants-1976_11 |