HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Decyl 7-[carbamoyl(4-hydroxynonyl)amino]heptanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | Diazodecane | HCID 15635947 | — |
| Reactant | 7-[Carbamoyl(4-hydroxynonyl)amino]heptanoic acid | HCID 21501441 | — |
| Reactant | 7-[Carbamothioyl(4-hydroxynonyl)amino]heptanoic acid | HCID 53968207 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Decyl 7-[carbamoyl(4-hydroxynonyl)amino]heptanoate | HCID 53798252 | — |
Reaction Steps
Using the method of Example 23 but substituting an ether solution of 1-diazodecane for the ether solution of diazomethane and 7-[1-(4-hydroxynonyl)ureido]heptanoic acid for 7-[1-(4-hydroxynonyl)thioureido]heptanoic acid, there is obtained decyl 7-[1-(4-hydroxynonyl)ureido]-heptanoate as a viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03989749 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-24c18fc8d3c649e8a56be662bc31e631 |
| Source note | uspto-grants-1976_11 |