2-Chloro-N,N-dimethylethylamine → HCID 21793851, compound

HRID 1729992Notes

Reaction equation

HRID 1729992 reaction equation
[CH3:1][O:2][C:3]1[C:4]([O:18][CH3:19])=[CH:5][C:6]2[C:15]3[CH2:14][CH2:13][NH:12][CH2:11][C:10]=3[C:9](=[O:16])[NH:8][C:7]=2[CH:17]=1.[CH3:20][N:21]([CH2:23][CH2:24]Cl)[CH3:22]>>[CH3:20][N:21]([CH3:22])[CH2:23][CH2:24][N:12]1[CH2:11][C:10]2[C:9](=[O:16])[NH:8][C:7]3[CH:17]=[C:3]([O:2][CH3:1])[C:4]([O:18][CH3:19])=[CH:5][C:6]=3[C:15]=2[CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 79012-Chloro-N,N-dimethylethylamineHCID 21793850HCID 21793850, compound

Product 1

HCID 21793851HCID 21793851, compound

Procedure

In the same way as described in example 10, 0.02 m of 1,2,3,4-tetrahydro-8,9-dimethoxybenzo[c][2,7]naphthyridin-5(6H)-one was alkylated with dimethylamino ethyl chloride. Crystallization from acetonitrile gave analytical material, mp 160°-164° C.

Workup

  1. customCrystallization from acetonitrile
  2. customgave analytical material, mp 160°-164° C.

Sources & evidence

ORD record
ord-6a80fc02cb784a44bba580a05e7ee993
Source dataset
uspto-grants-1976_11
Patent number
US03991064

Reaction notes

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