HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 54167955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | p-Chloro-n-propylbenzylamine | HCID 580714 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54167955 | HCID 54167955 | — |
Reaction Steps
A solution of 25.2 g. N-4-chlorobenzyl-N-propylamine in 150 ml. ethyl acetate was added to 150 ml. ethyl acetate under reflux whilst phosgene was passed through. The passage of phosgene was continued for 21/2 hours, after which the ethyl acetate was evaporated to give an oily product. Distillation gave N-4-chlorobenzyl-N-propylcarbamoyl chloride, an oil b.p. 162°-164° C./4.0 mm. Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03991071 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-bd96f1d19e3947468a944a5f697906c7 |
| Source note | uspto-grants-1976_11 |