3-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetate → HCID 22759281, compound

HRID 1730126Notes

Reaction equation

HRID 1730126 reaction equation
O1CCCCC1[O:7][CH2:8][C:9]#[C:10][CH:11]([O:21][C:22](=[O:24])[CH3:23])[CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1.O1CCCCC1OCCCC(OC(=O)C)COC1C=CC(F)=CC=1>>[C:22]([O:21][CH:11]([CH2:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([F:20])=[CH:16][CH:15]=1)[C:10]#[C:9][CH2:8][OH:7])(=[O:24])[CH3:23]

Participants

3

Reactant 2

HCID 227592583-Pentyn-2-ol, 1-(4-fluorophenoxy)-5-[(tetrahydro-2H-pyran-2-yl)oxy]-, 2-acetateHCID 22759299HCID 22759299, compound

Product 1

HCID 22759281HCID 22759281, compound

Procedure

This compound is prepared by the procedure described in Example 2, Step E, except that 1-(2 -tetrahydropyranyloxy)-4-acetoxy-5-(4-fluorophenoxy)-2-pentyne (Example 2, Step C) is substituted for 1-(2-tetrahydropyranyloxy)- 4-acetoxy-5-(4-fluorophenoxy)pentane. The subject compound is obtained as a light yellow oil which is not distilled but used directly in the next step.

Workup

  1. customThis compound is prepared by the procedure
  2. customThe subject compound is obtained as a light yellow oil which
  3. distillationis not distilled

Sources & evidence

ORD record
ord-3fb64aa0541d485da50744565691df21
Source dataset
uspto-grants-1976_11
Patent number
US03991106

Reaction notes

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