HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-[2-(3,4-Dimethoxyphenyl)ethyl]-4-(2-chlorobenzamido)-piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-{1-[2-(3,4-dimethoxyphenyl)ethyl]-4-piperidinyl}benzamide | HCID 21413257 | — |
| Product | 1-[2-(3,4-Dimethoxyphenyl)ethyl]-4-(2-chlorobenzamido)-piperidine | HCID 21430616 | — |
Reaction Steps
The title compound as its hydrochloride (m.P. 250°-2° C) was prepared in the same way as for the compound of Example 5 but using o-chlorobenzoyl chloride in place of benzoyl chloride. (Found: C, 60.2; H,6.1; N, 6.3. C22H27CiN2O3HCl requires C, 60.3; H, 6.2; N, 6.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992389 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-9e1b599320dd4ba08dffd06c4ee946a3 |
| Source note | uspto-grants-1976_11 |