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1,3-Benzodioxole-5-carbonyl chloride → 2-(3,4-Dimethoxyphenyl)ethyl-4-piperonylamidopiperidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Benzodioxole-5-carbonyl chloride | HCID 2734749 | — |
| 反応物 | N-{1-[2-(3,4-dimethoxyphenyl)ethyl]-4-piperidinyl}benzamide | HCID 21413257 | — |
| 生成物 | 2-(3,4-Dimethoxyphenyl)ethyl-4-piperonylamidopiperidine | HCID 21430636 | — |
| 生成物 | Dihydrate;hydrochloride | HCID 21899424 | — |
反応手順
The title compound hydrochloride dihydrate (m.p. 285°-8° C) was prepared in the same way as for the compound of Example 5 but utilising piperonyloyl chloride in place of benzoyl chloride. (Found: C, 57.1; H, 6.8; N, 5.7. C23H28N2O5.HCl.2H2O requires C, 57.0; H, 6.8; N, 5.8%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03992389 |
| 出典データセット | uspto-grants-1976_11 |
| ORD ID | ord-95a18aa2a5c44b859111d72bcc865d4e |
| 出典メモ | uspto-grants-1976_11 |