HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21430644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(3-Benzoylpropyl)-4-benzamidopiperidine | HCID 10089254 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21430644 | HCID 21430644 | — |
Reaction Steps
A solution of 4-benzamido-1-(4-phenyl-4-oxobutyl)-piperidine (1.75 g., 0.005 mole) and iodomethane (7.10 g., 0.05 mole) in N,N-dimethylformamide (5 ml.) was stirred for 150 hours at room temperature. The reaction mixture was filtered and the residue was washed with fresh N,N-dimethylformamide and then diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992389 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-963688f9ce3041d89b0a8c293bdd7271 |
| Source note | uspto-grants-1976_11 |