HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyltetradecylamine → 1-Adamantylcarbonylmethyldimethyltetradecylammonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyltetradecylamine | HCID 8211 | — |
| Reactant | Bromomethyl tricyclo[3.3.1.13,7]dec-1-yl ketone | HCID 197820 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Adamantylcarbonylmethyldimethyltetradecylammonium bromide | HCID 86733511 | 84.2% |
Reaction Steps
A mixture of 1.3g. (0.005 mole) 1-adamantyl bromomethyl ketone and 1.23g (0.005 mole) dimethyltetradecylamine was solubilized by the addition of 30cc acetone. The next day the solidified mixture was washed with ether and recrystallized from ethyl acetate to yield 2.1g white crystals, m.p. 134°-135.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992431 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-d8b975fbe5074eda8ae400398151140d |
| Source note | uspto-grants-1976_11 |