Cyclohexyl propionate → HCID 15817998, compound

HRID 1730442Notes

Reaction equation

HRID 1730442 reaction equation
C(O[CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][C:5]1=[O:10])C.[CH:11]1([O:17]C(=O)CC)CCCC[CH2:12]1.[H][H]>[Pd]>[CH2:11]([O:17][O:10][C:5]1[CH:4]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH3:12]

Participants

5

Reactant 3

HCID 61375Cyclohexyl propionateHCID 27333302-EthoxycyclohexanoneHCID 178418361HCID 178418361, compound

Product 1

HCID 15817998HCID 15817998, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

A solution of 10 gm. 2-ethoxycyclohexanone in 100 ml. cyclohexylpropionate was refluxed over 400 mg. of palladium on carbon until approximately 75% hydrogen had evolved. The catalyst was removed by filtration. O-ethoxyphenol was obtained in high yield.

Workup

  1. customThe catalyst was removed by filtration

Sources & evidence

ORD record
ord-ae19e5f7f1f54d7eb450cd8cda19c5c2
Source dataset
uspto-grants-1976_11
Patent number
US03992452

Reaction notes

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