HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 2,4-Difluoro-1,1'-biphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Reactant | 2,4-Difluoroaniline | HCID 9709 | — |
| Product | 2,4-Difluoro-1,1'-biphenyl | HCID 169974 | — |
Reaction Steps
To a 50 liter resin pot equipped with stirrer, thermometer, nitrogen-inlet, internal steam coil and reflux condenser is charged 31.5 liters of benzene, 1.025 liters of isoamyl nitrite and 700 g. (5.43 moles) of 2,4-difluoroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992459 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-01a9bc039a2043b18a83d8c5a4868aef |
| Source note | uspto-grants-1976_11 |