HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 178521125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178524727 | HCID 178524727 | — |
| Product | HCID 178521125 | HCID 178521125 | — |
Reaction Steps
A mixture of 9.2 g of 4-hydroxy-8-chloro-3-quinoline-carboxylic acid in 100ml of thionyl chloride was stirred at room temperature for 24 hours and wasthen vacuum filtered. The recovered precipitate was washed to obtain 0.4 g of 4 -hydroxy-8-chloro-3-quinoline-carboxylic acid chloride melting at 258° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992540 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-9cef5c047a8b46a893983bf2165fa5a8 |
| Source note | uspto-grants-1976_11 |