HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-methylthiazole → HCID 54695926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-methylthiazole | HCID 351770 | — |
| Reactant | 4-hydroxy-2-methyl-2H-naphtho[2,1-e]-1,2-thiazine-3-carboxylic acid methylester-1,1-dioxide | HCID 54690651 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54695926 | HCID 54695926 | 67% |
Reaction Steps
4-Hydroxy-2-methyl-N-(5-methyl-2-thiazolyl)-2H-naphtho[2,1-e]-1,2-thiazine-3-carboxamide-1,1-dioxide was prepared analogous to Example 22 from 4-hydroxy-2-methyl-2H-Naphtho[ 2,1-e]-1,2-thiazine-3-carboxylic acid methyl ester-1,1-dioxide and 2-amino-5-methyl-thiazole. Yield: 67% of theory, m.p. 249°-250° C (decomp.; from xylene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992535 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-1110e4b0d1fc4cf69583763dd9ee632d |
| Source note | uspto-grants-1976_11 |