HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-(Benzyloxy)piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-Acetyl-3-benzyloxypiperidine | HCID 20506119 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(Benzyloxy)piperidine | HCID 19960604 | — |
Reaction Steps
1-Acetyl-3-benzyloxypiperidine (0.043 mole), sodium hydroxide (0.086 mole) and water (30 ml.) are combined and refluxed for 24 hours. The reaction mixture is saturated with potassium carbonate and extracted three times with ether. The ether is removed by evaporation and the yellow oil is distilled at 92°-94° C. (0.3 mm Hg.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03992441 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-c002aabaeaa749658d097054ac7da928 |
| Source note | uspto-grants-1976_11 |