Veratryl chloride → HCID 54561794, compound

HRID 1730620Notes

Reaction equation

HRID 1730620 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:10]=1[O:11][CH3:12])[CH2:6]Cl.[N+:13]([C:16]1[O:20][C:19]([CH:21]=[CH:22][C:23]2[NH:24][CH:25]=[CH:26][N:27]=2)=[CH:18][CH:17]=1)([O-:15])=[O:14]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][C:10]=1[O:11][CH3:12])[CH2:6][N:27]1[CH:26]=[CH:25][N:24]=[C:23]1[CH:22]=[CH:21][C:19]1[O:20][C:16]([N+:13]([O-:15])=[O:14])=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 81740Veratryl chlorideHCID 286751HCID 286751, compound

Product 1

HCID 54561794HCID 54561794, compound

Procedure

Using the same general procedure as employed in Example 1, the captioned compound was prepared from 3,4-dimethoxybenzyl chloride (as prepared from the corresponding alcohol) in lieu of the 2,3-dimethoxybenzyl chloride intermediate of Example 1.

Sources & evidence

ORD record
ord-5680ed8a6c064fcc9d777764a72c431c
Source dataset
uspto-grants-1976_11
Patent number
US03993643

Reaction notes

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