3-Methoxybenzyl chloride → HCID 54047392, compound

HRID 1730621Notes

Reaction equation

HRID 1730621 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH2:6]Cl.[N+:11]([C:14]1[O:18][C:17]([CH:19]=[CH:20][C:21]2[NH:22][CH:23]=[CH:24][N:25]=2)=[CH:16][CH:15]=1)([O-:13])=[O:12]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:8]=[CH:9][CH:10]=1)[CH2:6][N:25]1[CH:24]=[CH:23][N:22]=[C:21]1[CH:20]=[CH:19][C:17]1[O:18][C:14]([N+:11]([O-:13])=[O:12])=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 699943-Methoxybenzyl chlorideHCID 286751HCID 286751, compound

Product 1

HCID 54047392HCID 54047392, compound

Procedure

Using the same general procedure of Example 1, the captioned compound was prepared using 3-methoxybenzyl chloride and 2-[2-(5-nitro-2-furyl)vinyl]imidazole. After recrystallization from ethanol water the product melted at 143°-145°.

Workup

  1. customthe captioned compound was prepared
  2. customAfter recrystallization from ethanol water the product melted at 143°-145°

Sources & evidence

ORD record
ord-fc1451f5bd6a459ba34ee3f0093a75f0
Source dataset
uspto-grants-1976_11
Patent number
US03993643

Reaction notes

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