Benzene, (3-bromopropoxy)- → 2-[2-(5-Nitrofuran-2-yl)ethenyl]-1-(3-phenoxypropyl)-1H-imidazole

HRID 1730624Notes

Reaction equation

HRID 1730624 reaction equation
[O:1]([CH2:8][CH2:9][CH2:10]Br)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+:12]([C:15]1[O:19][C:18]([CH:20]=[CH:21][C:22]2[NH:23][CH:24]=[CH:25][N:26]=2)=[CH:17][CH:16]=1)([O-:14])=[O:13]>>[O:1]([CH2:8][CH2:9][CH2:10][N:26]1[CH:25]=[CH:24][N:23]=[C:22]1[CH:21]=[CH:20][C:18]1[O:19][C:15]([N+:12]([O-:14])=[O:13])=[CH:16][CH:17]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 68522Benzene, (3-bromopropoxy)-HCID 286751HCID 286751, compound

Product 1

HCID 541479812-[2-(5-Nitrofuran-2-yl)ethenyl]-1-(3-phenoxypropyl)-1H-imidazole

Procedure

Using the same general procedure of Example 1, the captioned compound was prepared using 3-phenoxypropyl bromide and 2-[2-(5-nitro-2-furyl)vinyl]imidazole. The resulting orange product after recrystallization from ethanol-water melted at 85°-86°.

Workup

  1. customthe captioned compound was prepared
  2. customThe resulting orange product after recrystallization from ethanol-water melted at 85°-86°

Sources & evidence

ORD record
ord-99caa3a4287a421b8259e80a4f509c54
Source dataset
uspto-grants-1976_11
Patent number
US03993643

Reaction notes

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