4-Methoxybenzyl bromide → HCID 149265, compound

HRID 1730625Notes

Reaction equation

HRID 1730625 reaction equation
[N+:1]([C:4]1[O:8][C:7]([CH:9]=[CH:10][C:11]2[NH:12][CH:13]=[CH:14][N:15]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH3:16][O:17][C:18]1[CH:25]=[CH:24][C:21]([CH2:22]Br)=[CH:20][CH:19]=1>>[CH3:16][O:17][C:18]1[CH:25]=[CH:24][C:21]([CH2:22][N:12]2[CH:13]=[CH:14][N:15]=[C:11]2[CH:10]=[CH:9][C:7]2[O:8][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 1650214-Methoxybenzyl bromideHCID 286751HCID 286751, compound

Product 1

HCID 149265HCID 149265, compound

Procedure

Using the same general procedure of Example 1, the captioned compound was prepared using 2-[2-(5-nitro-2-furyl)vinyl]imidazole and 4-methoxybenzyl bromide. Recrystallization from benzene-ethanol gave an orange solid, mp 151°-152°.

Workup

  1. customthe captioned compound was prepared
  2. customRecrystallization from benzene-ethanol
  3. customgave an orange solid, mp 151°-152°

Sources & evidence

ORD record
ord-46fe90e1ba8a4c6ca14ee330d8573158
Source dataset
uspto-grants-1976_11
Patent number
US03993643

Reaction notes

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