HCID 21496269, compound → HCID 21496255, compound

HRID 1730738Notes

Reaction equation

HRID 1730738 reaction equation
[OH:1][CH2:2][CH2:3][S:4][CH2:5][CH:6]([C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2F)=[CH:10][CH:9]=1)[OH:7]>C1C=CC=CC=1.C(OCC)(=O)C>[OH:1][CH2:2][CH2:3][S:4][CH2:5][CH:6]([C:8]1[CH:13]=[CH:12][C:11]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH:10][CH:9]=1)[OH:7]

Participants

3

Reactant 1

HCID 21496269HCID 21496269, compound

Product 1

HCID 21496255HCID 21496255, compound

Reagents, catalysts & solvents 1

HCID 21583983Benzene ethyl acetateSolvent

Procedure

2-Hydroxyethyl-[2-(2'-fluoro-4-biphenylyl)-2-hydroxyethyl]-sulfide, an oil, Rf -value: 0.3 on silicagel-polygram-plates with benzene/ethyl acetate = 1:1 as the eluant, was prepared in analogous manner.

Sources & evidence

ORD record
ord-4dc839107aa74e64a6cdd395e1b30502
Source dataset
uspto-grants-1976_11
Patent number
US03993683

Reaction notes

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