HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 131710530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | HCID 15573409 | HCID 15573409 | — |
| Reactant | HCID 178418348 | HCID 178418348 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 131710530 | HCID 131710530 | — |
Reaction Steps
According to the procedure described by Example 4, 479 mg. of 2,2,2-trichloroethyl 3-methyl-7-phenoxyacetamido-3-cephem-4-carboxylate was reacted with methanol, methyl lithium and t-butyl hypochlorite in anhydrous tetrahydrofuran at -80° C. to provide 2,2,2-trichloroethyl 3-methyl-7-methoxy-7-phenoxy-acetamido-3-cephem-4-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994885 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-383f7e37163042789f899216d2f43956 |
| Source note | uspto-grants-1976_11 |