HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-enoyl chloride → HCID 131710542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Reactant | 4-[2-(Dimethylamino)ethoxy]aniline | HCID 6484655 | — |
| Product | HCID 131710542 | HCID 131710542 | 100.3% |
Reaction Steps
The reaction between 27.0g of 4-[2-(dimethylamino)-ethoxy]benzenamine and 24.9g of cinnamoyl chloride (using the procedure of Example 4, part b) gives 52.0g of crystals, melting point 257°-259° C, dec. Crystallization from a solution of 500 ml of methanol and 30 ml of water yields 43.1g of product, melting point 263°-265° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994900 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-204a412e6e2e4434b51476aa30c65840 |
| Source note | uspto-grants-1976_11 |