HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 1-(3-Pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Pyrinuron | HCID 40813 | — |
| Solvent | Dimethyl Ether | HCID 8254 | — |
| Product | 1-(3-Pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide | HCID 20368872 | 76% |
Reaction Steps
Gaseous HBr was passed into a solution of 3 g. of 3-pyridylmethyl-3-(4-nitrophenyl)urea in the monomethyl ether of ethyleneglycol. Ether was added to give a precipitate and after isolation, washing with ether and drying, 2.95 g. of white solid was obtained. This was a 76% yield of 1-(3-pyridylmethyl)-3-(4-nitrophenyl)urea hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994905 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-c90e0c80e13f467ab0012d87ee8db524 |
| Source note | uspto-grants-1976_11 |