HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-3-phenyl-1H-indazole → 1-Dimethylaminoethyl-3-phenyl-5-methylindazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-3-phenyl-1H-indazole | HCID 610412 | — |
| Reactant | N,N-Dimethylaminoethyl chloride hydrochloride | HCID 11636816 | — |
| Product | 1-Dimethylaminoethyl-3-phenyl-5-methylindazole hydrochloride | HCID 68141044 | 63.2% |
Reaction Steps
By the procedure similar to that described in Example 1, 3-phenyl-5-methylindazole (4.17 g) and dimethylaminoethyl chloride hydrochloride (4.32 g) were treated to obtain 4.0 g of 1-dimethylaminoethyl-3-phenyl-5-methylindazole hydrochloride (m.p. 191°-192° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994890 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-369363b8034644fa9c09bbd46e2bfb65 |
| Source note | uspto-grants-1976_11 |