HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-(diethylamine)ethane hydrochloride → 1-Diethylaminoethyl-3-phenyl-5-methylindazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| Reactant | 5-Methyl-3-phenyl-1H-indazole | HCID 610412 | — |
| Product | 1-Diethylaminoethyl-3-phenyl-5-methylindazole hydrochloride | HCID 68139155 | 58.1% |
Reaction Steps
By the procedure similar to that described in Example 1, 3-phenyl-5-methylindazole (4.17 g) and diethylaminoethyl chloride hydrochloride (5.16 g) were treated to obtain 4.0 g of 1-diethylaminoethyl-3-phenyl-5-methylindazole hydrochloride (m.p. 131°-133° C).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994890 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-4783d40908c84f29aec782ea65d159a4 |
| Source note | uspto-grants-1976_11 |