1-Chloro-2-(diethylamine)ethane hydrochloride → HCID 68139505, compound

HRID 1730927Notes

Reaction equation

HRID 1730927 reaction equation
[C:1]1([C:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[NH:9][N:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH2:17]([N:19]([CH2:22][CH2:23][Cl:24])[CH2:20][CH3:21])[CH3:18]>>[ClH:24].[CH2:17]([N:19]([CH2:22][CH3:23])[CH:20]([C:14]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:15]=1[C:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[N:8][NH:9]2)[CH3:21])[CH3:18]

Participants

3

Reactant 2

HCID 133631-Chloro-2-(diethylamine)ethane hydrochlorideHCID 3003853-phenyl-1H-indazole

Product 1

HCID 68139505HCID 68139505, compoundYield 30.4%

Procedure

By the procedure similar to that described in Example 1, 3-phenylindazole (3.88 g) and diethylaminoethyl chloride hydrochloride (5.16 g) were treated to obtain 2.0 g of 1-diethylaminoethyl-3-phenylindazole hydrochloride (m.p. 114°-118° C).

Workup

  1. additionwere treated

Sources & evidence

ORD record
ord-3aaa136a86c54394b7aac7929e63a4b6
Source dataset
uspto-grants-1976_11
Patent number
US03994890

Reaction notes

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