3-(Dimethylamino)propyl chloride hydrochloride → HCID 68139135, compound

HRID 1730928Notes

Reaction equation

HRID 1730928 reaction equation
[C:1]1([C:7]2[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[NH:9][N:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH3:17][N:18]([CH2:20][CH2:21][CH2:22][Cl:23])[CH3:19]>>[ClH:23].[CH3:17][N:18]([CH3:19])[CH:20]([C:14]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:15]=1[C:7]([C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1)=[N:8][NH:9]2)[CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 943083-(Dimethylamino)propyl chloride hydrochlorideHCID 3003853-phenyl-1H-indazole

Product 1

HCID 68139135HCID 68139135, compoundYield 55.5%

Procedure

By the procedure similar to that described in Example 1, 3-phenylindazole (3.88 g) and dimethylaminopropyl chloride hydrochloride (4.74 g) to obtain 3.5 g of 1-dimethylaminopropyl-3-phenylindazole hydrochloride (m.p. 140°-143° C).

Sources & evidence

ORD record
ord-9481e5ec70144a35b3e1c85f06424d23
Source dataset
uspto-grants-1976_11
Patent number
US03994890

Reaction notes

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