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HRID1730929

反应详情

EQUATION

反应方程式

HRID 1730929 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCCCl.Cl
HCID94308

Dimethylaminopropyl chloride hydrochloride

C5H13Cl2N

结构：Clc1ccc2[nH]nc(-c3ccccc3)c2c1
HCID615118

5-Chloro-3-phenyl-1H-indazole

C13H9ClN2

PRODUCTS

生成物

1
结构：CCC(c1c(Cl)ccc2[nH]nc(-c3ccccc3)c12)N(C)C.Cl
HCID68139842

未命名化合物

收率 135.4%

PROCEDURE

实验过程

By the procedure similar to that described in Example 1, 3-phenyl-5-chloroindazole (4.57 g) and dimethylaminopropyl chloride hydrochloride (4.74 g) were treated to obtain 4.74 g of 1-dimethylaminopropyl-3-phenyl-5-chloroindazole hydrochloride (m.p. 158°-160° C).

WORKUP

后处理

  1. additionwere treated