3-(Dimethylamino)propyl chloride hydrochloride → HCID 131710544, compound

HRID 1730930Notes

Reaction equation

HRID 1730930 reaction equation
[C:1]1([C:7]2[C:15]3[C:10](=[CH:11][CH:12]=[C:13]([Br:16])[CH:14]=3)[NH:9][N:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.CN(CCC[Cl:24])C>>[ClH:24].[C:1]1([C:7]2[C:15]3[C:10](=[CH:11][CH:12]=[C:13]([Br:16])[CH:14]=3)[NH:9][N:8]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 943083-(Dimethylamino)propyl chloride hydrochlorideHCID 6234155-Bromo-3-phenyl-1H-indazole

Product 1

HCID 131710544HCID 131710544, compound

Procedure

By the procedure similar to that described in Example 1, 3-phenyl-5-bromoindazole (4.10 g) and dimethylaminopropyl chloride hydrochloride (3.56 g) were treated to obtain 4.0 g of 1-dimethylaminopropyl)-3-phenyl-5-bromoindazole hydrochloride (m.p. 149°-150° C).

Workup

  1. additionwere treated

Sources & evidence

ORD record
ord-7074ac806a1a476297f2c027ea31240d
Source dataset
uspto-grants-1976_11
Patent number
US03994890

Reaction notes

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