5-Methyl-3-phenyl-1H-indazole → HCID 68140693, compound

HRID 1730937Notes

Reaction equation

HRID 1730937 reaction equation
[C:1]1([C:7]2[C:15]3[C:10](=[CH:11][CH:12]=[C:13]([CH3:16])[CH:14]=3)[NH:9][N:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:17]([N:20]([CH2:24][CH2:25][CH2:26][Cl:27])[CH2:21][CH:22]=[CH2:23])[CH:18]=[CH2:19]>>[ClH:27].[CH2:17]([N:20]([CH2:21][CH:22]=[CH2:23])[CH:24]([C:14]1[C:13]([CH3:16])=[CH:12][CH:11]=[C:10]2[C:15]=1[C:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[N:8][NH:9]2)[CH2:25][CH3:26])[CH:18]=[CH2:19]

Participants

3

Reactant 2

HCID 6104125-Methyl-3-phenyl-1H-indazoleHCID 13706059HCID 13706059, compound

Product 1

HCID 68140693HCID 68140693, compoundYield 56.2%

Procedure

By the procedure similar to that described in Example 13, 3-phenyl-5-methylindazole (4.17 g) and diallylaminopropyl chloride (4.17 g) were treated to obtain 4.3 g of 1-diallylaminopropyl-3-phenyl-5-methylindazole hydrochloride (m.p. 81°-82° C).

Workup

  1. additionwere treated

Sources & evidence

ORD record
ord-73f3cfd0661249c2a8bc5d6de5864687
Source dataset
uspto-grants-1976_11
Patent number
US03994890

Reaction notes

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