HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazoethane → HCID 54342882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazoethane | HCID 70695 | — |
| Reactant | 4-[(Pyridin-2-yl)oxy]benzoyl chloride | HCID 21494428 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54342882 | HCID 54342882 | — |
Reaction Steps
To a solution of 4-(2-pyridyloxy)benzoyl chloride in ether, a solution of diazoethane in ether is added dropwise, and the reaction is effected as in Example 8 (2) to give 4-(2-pyridyloxy)-1-(2-diazopropionyl)benzene (4.72 g). This substance is recrystallized from ethyl acetate to give crystals melting at 101° to 102° C (decomp.). IR (CCl4): 2070, 1630, 1590 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994908 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-b585ad5ff2704b3f8647fbd71940583e |
| Source note | uspto-grants-1976_11 |