HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68142397, compound → HCID 21494544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68142397 | HCID 68142397 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21494544 | HCID 21494544 | — |
Reaction Steps
A solution was prepared of 2,4-dimethyl-4-isopropyl-5-(bromomethylene)-2-oxazolinium bromide in ethanol and allowed to stand at room temperature. The solvent gradually evaporated and the solid residue was recrystallized from ethanol to yield 1-bromo-3,4-dimethyl-3-amino-2-pentanone hydrobromide having a melting point of about 158°-160° C. The material was identified by the n.m.r. spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994917 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-1a8b461a57d346279feee9cb346a83d0 |
| Source note | uspto-grants-1976_11 |