HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → 9-Phenyl-1,2,3,9b-tetrahydro-5H-imidazo[2,1-a]isoindol-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | 2-Benzoylbenzoic Acid | HCID 6813 | — |
| Product | 9-Phenyl-1,2,3,9b-tetrahydro-5H-imidazo[2,1-a]isoindol-5-one | HCID 21494586 | — |
Reaction Steps
Reflux 45 g. of o-benzoylbenzoic acid and 120 ml. of ethylenediamine for 3 hours. Pour the mixture into ice water, allow to stand until the mixture is at room temperature and separate the product by filtration. Recrystallize from ethanol to obtain 9-phenyl-1,2,3,9b-tetrahydro-5H-imidazo-[2,1-a]isoindol-5-one, m.p. 155°-7° C. Elemental analysis confirms the empirical formula C16H14N2O.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994920 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-06aa031440834019bcb830f0cb77c577 |
| Source note | uspto-grants-1976_11 |