HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 12907015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 13554730 | HCID 13554730 | — |
| Product | HCID 12907015 | HCID 12907015 | — |
Reaction Steps
Condense 3-benzyl-3-hydroxyphthalide (15 g.) and ethylenediamine (30 ml.) by the procedure of Example 1 to obtain 9b-benzyl-1,2,3,9b-tetrahydro-5H-imidazo[2,1-a]isoindol-5-one, m.p. 115°-117° C. (elemental analysis confirms the empirical formula C17H16N2O), reduce with lithium aluminum hydride and treat with hydrogen chloride as described in Example 1 to obtain 1-benzyl-1,2,3,4,5,6-hexahydro-2,5-benzodiazocine dihydrochloride, m.p. 238°-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994920 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-5070152ebd58451389fc21f7fb1925fe |
| Source note | uspto-grants-1976_11 |