HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Ethoxyacetophenone → Methyl 2-[4-(2-p-ethoxybenzoylethenyl)phenoxy]-2-methyl-2 ethylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Ethoxyacetophenone | HCID 72872 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Methyl 2-(4-formylphenoxy)-2-methylbutanoate | HCID 21494898 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 2-[4-(2-p-ethoxybenzoylethenyl)phenoxy]-2-methyl-2 ethylacetate | HCID 54024537 | — |
Reaction Steps
Following the procedure in Example 1 using 7.1 parts of methyl 2-(4-formylphenoxy)-2-methyl-2-ethylacetate and 4.9 parts of p-ethoxyacetophenone in 10 parts by volume of ethanol containing 0.1 part of sodium metal provides methyl 2-[4-(2-p-ethoxybenzoylethenyl)phenoxy]-2-methyl-2 ethylacetate. This compound has the following structural formula. ##SPC11##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994955 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-3ab079da03ff4dfb9d3b16111d39397c |
| Source note | uspto-grants-1976_11 |