HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide → HCID 21494728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | Diethyl azodicarboxylate | HCID 5462977 | — |
| Reactant | HCID 21494763 | HCID 21494763 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21494728 | HCID 21494728 | — |
Reaction Steps
In the manner given in Example 1B, 2'-chloro-2-[3-[2-(dimethylamino)ethyl]-5-(hydroxymethyl)-4H-1,2,4-triazol-4-yl]benzophenone in tetrahydrofuran is treated with phthalimide, triphenylphosphine and diethylazodicarboxylate to give 2'-chloro-2-[3-[2-(dimethylamino)-ethyl]-5-(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994940 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-c99fb066b2324889a34e5870f2f8f3f0 |
| Source note | uspto-grants-1976_11 |