HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalimide → HCID 21494777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | HCID 21494746 | HCID 21494746 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21494777 | HCID 21494777 | — |
Reaction Steps
In the manner given in Example 1B, 5-chloro-2',6'-difluoro-2-[3-[2-(dimethylamino)ethyl]-5-(hydroxymethyl)-4H-1,2,4-triazol-4-yl]benzophenone in methylene chloride is treated with phthalimide, triphenylphosphine and diethyl azodicarboxylate to give 5-chloro-2',6'-difluoro-2-[3-[2-(dimethylamino)ethyl]-5-(phthalimidomethyl)-4H-1,2,4-triazol-4-yl]benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03994940 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-680a34ae56a946c3a22e4764882d05f8 |
| Source note | uspto-grants-1976_11 |