HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 21495113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | 2-Bromo-4-chloro-1-[(chloromethyl)sulfanyl]benzene | HCID 21495132 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21495113 | HCID 21495113 | 85.9% |
Reaction Steps
To a solution of 18.8 g of 2-aminopyridine in 180 ml of benzene is added 54.6 g of the product from example 30, and the mixture stirred and heated under reflux for about twelve hours. The cooled mixture is filtered to give about 62.8 g of the named compound, mp about 240°-242°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995042 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-e9d73cd651c041f58533f87b672254eb |
| Source note | uspto-grants-1976_11 |