HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 21495354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | Ethyl pyruvate | HCID 12041 | — |
| Reactant | 2-(1H-Inden-2-yl)ethan-1-ol | HCID 14316626 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21495354 | HCID 21495354 | — |
Reaction Steps
Indene-2-ethanol (3.5 g) described in Examples 474 and 476, is treated with ethyl pyruvate (4 g) and boron trifluoride-etherate (2 ml) in benzene (50 ml) according to the procedure of Example 2 to yield the title compound, m.p. 171°-173° C., νmaxnujol 1720 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995052 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-e4e7817a736048b285535d960c98cccc |
| Source note | uspto-grants-1976_11 |