HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(3'-p-Chlorobenzoyl-phenyl)-propionyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(3'-p-Chlorobenzoyl-phenyl)-propionic acid | HCID 21495624 | — |
| Product | 3-(3'-p-Chlorobenzoyl-phenyl)-propionyl chloride | HCID 21495647 | — |
Reaction Steps
6.96 g of 3-(3'-p-chlorobenzoyl-phenyl)-propionic acid and 70 ml of thionyl chloride were refluxed for 3 hours and then evaporated to dryness. The residue was taken up in 100 ml of benzene and evaporated to dryness to obtain 8.7 g of 3-(3'-p-chlorobenzoyl-phenyl)-propionyl chloride which was used as is.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03995056 |
| Source dataset | uspto-grants-1976_11 |
| ORD ID | ord-1bc2fd2824964c54b99759e710fdc4a9 |
| Source note | uspto-grants-1976_11 |