Ethyl Acetoacetate → HCID 13670854, compound

Participants

Reaction Steps

0.8 g (6 mmol) of 3-cyanobenzaldehyde, 0.8 g (6 mmol) of ethyl acetoacetate and 1.6 g (6 mmol) of 6-amino-2,4-dimorpholino-pyrimidine were heated together in 20 ml of ethanol for 15 hours under reflux. The reaction mixture was then cooled, and the precipitated product was filtered off with suction and recrystallized from a little ethanol, melting point: 210° C. Yield: 1.8 g (61%).

Provenance & Evidence