2-Aminopyridine → Benzothiazolone

HRID 1731329노트

반응식

HRID 1731329 반응식
BrC(C)C([C:5]1[CH:6]=[CH:7][C:8]2[S:12][C:11](=[O:13])[NH:10][C:9]=2[CH:14]=1)=O.NC1C=CC=CN=1>C(O)C>[S:12]1[C:8]2[CH:7]=[CH:6][CH:5]=[CH:14][C:9]=2[NH:10][C:11]1=[O:13]

참가 물질

4

반응물 2

HCID 104392-AminopyridineHCID 202287105-(2-Bromopropanoyl)-1,3-benzothiazol-2(3H)-one

생성물 1

HCID 13625Benzothiazolone수율 70.8%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

5-(3-Methylimidazo[1,2-? ? pyridin-2-yl)2-benzothiazolinone (1.07 g) was prepared in the substantially same manner as that of Example 2 from 5-(2-bromopropionyl)-2-benzothiazolinone (2.86 g) and 2-aminopyridine (2.8 g). mp.>290° C.(from aqueous ethanol),

출처 및 근거

ORD 기록
ord-afd6ba85adc44f448bc717f61a44ce5c
출처 데이터셋
uspto-grants-1986_11
특허 번호
US04621084

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