HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 131714943, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 13657320 | HCID 13657320 | — |
| Reactant | HCID 14129901 | HCID 14129901 | — |
| Product | HCID 131714943 | HCID 131714943 | — |
Reaction Steps
The ester product from part (c) (2.7 g., 7.17 mmole) is treated for 1.5 hours with 10 ml. of trifluoroacetic acid and 1.6 ml. of anisole. After concentrating to dryness it is triturated with ether-hexane. The crude material is crystallized from ether to yield 2 g. of 1-[[(2-carboxyethyl)methylamino]carbonyl]-L-proline, phenylmethyl ester; m.p. 102°-104°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04621092 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-4aa8bac342764236b60cda2d6b989ea0 |
| Source note | uspto-grants-1986_11 |