HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Benzoylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Chromic Acid | HCID 24425 | — |
| Reactant | 3-(Hydroxymethyl)benzophenone | HCID 12783739 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-Benzoylbenzaldehyde | HCID 13020168 | — |
Reaction Steps
3-Benzoylbenzyl alcohol (2.0 g) in acetone (10 ml) was treated dropwise at 15°-20° C. with chromic acid solution. After stirring for 5 minutes, water (50 ml) was added and the mixture extracted with ether. The ethereal solution was washed with saturated Na2CO3, saturated NaCl, dried (Na2SO4), evaporated and distilled; b.p. 160°-170° C./0.08 mm, (1.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04622337 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-e20b1ccc6f8141a4bd663b6beff6ebe7 |
| Source note | uspto-grants-1986_11 |