3-Chloromandelic acid → HCID 20227974, compound

HRID 1731585Notes

Reaction equation

HRID 1731585 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]([OH:9])[C:6]([OH:8])=O.[CH3:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([CH2:21][CH2:22][C:23]([CH3:26])([CH3:25])[NH2:24])=[CH:17][CH:16]=1>>[CH3:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([CH2:21][CH2:22][C:23]([NH:24][C:6](=[O:8])[CH:5]([OH:9])[C:4]2[CH:10]=[CH:11][CH:12]=[C:2]([Cl:1])[CH:3]=2)([CH3:25])[CH3:26])=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 859813-Chloromandelic acidHCID 11019715HCID 11019715, compound

Product 1

HCID 20227974HCID 20227974, compound

Procedure

The title compound was prepared from 3-chloromandelic acid (2.1 g) and 3-(4-methoxyphenyl)-1,1-dimethylpropanamine (1.9 g) by an analogous procedure to that described in Description 12 and used without further purification.

Workup

  1. customused without further purification

Sources & evidence

ORD record
ord-1f90f7ac92fb4724884e70018da75278
Source dataset
uspto-grants-1986_11
Patent number
US04622342

Reaction notes

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