Triethylamine → HCID 14705811, compound

Participants

Reaction Steps

To a solution of (E)-3-chloroacrylonitrile (0.1 g) in tetrahydrofuran (2 ml) were added triphenylmethanethiol (0.332 g) and triethylamine (0.175 ml) under ice-cooling. The mixture was stirred at ambient temperature for 16 hours and poured into ice-water. The mixture was extracted with ethyl acetate. The extract was washed with brine, dried over magnesium sulfate and evaporated in vacuo to give (E)-3-tritylthioacrylonitrile (0.37 g).

Provenance & Evidence