HCID 13258487, compound → HCID 13469150, compound

HRID 1731716Notes

Reaction equation

HRID 1731716 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:9]2[S:10][CH:11]=[CH:12][CH:13]=2)=[CH:6][C:7]=1[CH3:8].ClC1N=NC(C2C=CC=CC=2)=C(C)C=1C.[CH3:29][N:30](C)[C:31]1N=NC(C2C=CSC=2)=CC=1C>>[CH3:29][N:30]([CH3:31])[C:2]1[N:3]=[N:4][C:5]([C:9]2[S:10][CH:11]=[CH:12][CH:13]=2)=[CH:6][C:7]=1[CH3:8]

Participants

4

Reactant 3

HCID 13258487HCID 13258487, compoundHCID 20226916HCID 20226916, compoundHCID 20226919HCID 20226919, compound

Product 1

HCID 13469150HCID 13469150, compound

Procedure

The above-named compound is prepared in the same manner as described for the aminopyridazines of Example 38, excepting that 3-chloro-4-methyl-6-(2-thienyl)pyridazine is substituted for 3-chloro-4,5-dimethyl-6-phenylpyridazine. The product obtained has a melting point of 50°-52° C. 3-(Dimethylamino)-4-methyl-6-(3-thienyl)pyridazine, a red oil, (Example 51a) is made in the same manner as described above for the 2-thienyl derivative.

Workup

  1. customThe above-named compound is prepared in the same manner
  2. customThe product obtained

Sources & evidence

ORD record
ord-80acaf92a7384ca3afa3f2ccc0cc0e5a
Source dataset
uspto-grants-1986_11
Patent number
US04623376

Reaction notes

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