HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Butylbenzylamine → N-Benzyl-N-butyl-N'-(3-chlorophenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Butylbenzylamine | HCID 75467 | — |
| Reactant | Phenyl hydrogen (3-chlorophenyl)carbonimidate | HCID 232110 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-Benzyl-N-butyl-N'-(3-chlorophenyl)urea | HCID 13733049 | — |
Reaction Steps
A solution of 1.46 g of phenyl N-(3-chlorophenyl)carbamate in 15 ml of tetrahydrofuran was added to a solution of 1.92 g of N-benzyl-n-butylamine in 20 ml of tetrahydrofuran and the mixture stirred under reflux for 24 hours. The mixture was diluted with hexane and the precipitate collected by filtration. Recrystallization from pentane afforded 1-benzyl-1-(n-butyl)-3-(3-chlorophenyl)urea, m.p. 69°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04623662 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-b2531c9fc7a9451e8ef34dde53f31da5 |
| Source note | uspto-grants-1986_11 |