HRID1731892

反应详情

EQUATION

反应方程式

HRID 1731892 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a stirred mixture of 100 ml of 10% aqueous sodium hydroxide and 100 ml of dichloromethane was added 15 g of 3-(3-methoxyphenyl)piperidine hydrochloride. After a few minutes, the layers were separated and the organic layer was dried using potassium carbonate. Evaporation of the dichloromethane solution then afforded 12.6 g of the title compound as an oil.

WORKUP

后处理

  1. waitAfter a few minutes
  2. customthe layers were separated
  3. customthe organic layer was dried
  4. customEvaporation of the dichloromethane solution