HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13687205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2-Acetylcyclohexanone | HCID 13400 | — |
| Reactant | HCID 13629447 | HCID 13629447 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 13687205 | HCID 13687205 | 38.2% |
Reaction Steps
In the same manner as in Example 4 but using 4-chloro-2-fluoro-5-nitrophenylhydrazine (4 g), 2-acetylcyclohexanone (2.8 g), a catalytic amount of acetic acid and xylene (10 ml), there was produced 2.3 g of 2-(4-chloro-2-fluoro-5-nitrophenyl)-3-methyl-4,5,6,7-tetrahydro-2H-indazole. m.p., 143°-144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04624699 |
| Source dataset | uspto-grants-1986_11 |
| ORD ID | ord-120cf4c309e743d28cc48e9f0c7211d3 |
| Source note | uspto-grants-1986_11 |